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Fig 5. C18-HPLC separation of thiosulphinate standards

(Supelco LC-18 250 x 4.6 mm column, methanol/water (50-50), 1.0 ml/min, 254 nm) (1) dimethyl, (2) allyl methyl + methyl allyl, (3) methyl 1-propenyl + 1-propenyl methyl, (4),(5) propyl methyl/methyl propyl, (6) diallyl, (7) allyl 1-propenyl, (8) 1-propenyl allyl + allyl 1-propyl (9) propyl allyl, (10) di-1-propenyl, (11) dipropyl.